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Beneficiation techniques include crushing, screening of particulates, and concentration (which involves the separation of valuable minerals from the other raw materials received from a grinding mill) and washing, In large-scale operations, various distinguishing properties of the minerals to be separated (e.g., magnetism, wettability, density ...

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The process involves first converting the α -spodumene into β -spodumene in a kiln at 1100 °C before grinding and mixing with sulphuric acid and roasting at 250 °C before water leaching at 90 °C, solution purification through neutralisation and …

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Similar aspects were described by [37] for Neoproterozoic spodumene pegmatites from southern Natal, South Africa. In the Iberian Peninsula, some petalite-rich pegmatites exhibit a similar texture [e.g. 38] named as SQUI [39] characterized by symplectic or fibrous intergrowths of spodumene + quartz due to the breakdown of petalite.

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β-spodumene. The α-spodumene is virtually refractory to hot acids. As a result of the phase transformation, the spodumene crystal structure expands by about 30% and becomes amenable to hot sulphuric acid attack. Due to this expansion, the specific gravity of the spodumene decreases from 3.1 g/cm3 (natural α-spodumene) to around 2.4 g/

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The β-form of spodumene is less dense (2.41 g.cm −3) because of its zeolite-like crystallographic structure that embeds nano-channels of about 3 Åin free diameter. This is when the lithium in the crystal structure is replaced by hydrogen or sodium which explains the ion exchange and better crushability or grinding properties of β-spodumene.

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